Synthesis and Crystal Structure Analysis of
Monocyclic ÃƒÅ½Ã‚Â²-Lactam Derivatives

Alam S; Hasan P; Aneja B; Md Ahmad B; Yadava U; Daniliuc CG; Abid M

Abstract

Synthesis and Crystal Structure Analysis of Monocyclic ÃÆÃÂ½ÃâÃÂ²-Lactam Derivatives

ÃÆÃÂ¯ÃâÃÂ»ÃâÃÂ¿Single crystals of monocyclic β-lactam derivatives, I and II were grown by slow evaporation method at room temperature. Crystallographic data set for I (C24H23NO3 ) was collected with D8 Venture Dual Source 100 CMOS diffractometer at 100K using ÃÆÃÂÃâÃ¢â¬Â¢ and ω scans methods while that for II (C32H26N2 O2 ) was collected with a Nonius Kappa CCD diffractometer. Single crystal X-ray diffraction analysis revealed that both compounds I and II crystallize in monoclinic crystal system with space group P21/c. The final R-factors for model structures were converged to 3.79 and 5.72%, respectively.ÃÆÃÂ¯ÃâÃÂ»ÃâÃÂ¿

Author(s):

Alam S, Hasan P, Aneja B, Md Ahmad B , Yadava U , Daniliuc CG and Abid M

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